Compound | RIcalc | RIlit | 30 dpia | 60 dpia | 90 dpia | |||
---|---|---|---|---|---|---|---|---|
Control | AMF | Control | AMF | Control | AMF | |||
n-Octane | 782 | 800 | 2.43 ± 1.18 | 0.10 ± 0.10 | 0.03 ± 0.04 | 0.14 ± 0.04 | ||
α-Thujene | 918 | 924 | 0.13 ± 0.23 | 0.46 ± 0.14 | 0.27 ± 0.37 | 0.33 ± 0.10 | ||
Camphene | 934 | 946 | 0.39 ± 0.42 | 0.07 ± 0.13 | 1.06 ± 0.94 | 1.86 ± 0.45 | 2.77 ± 0.40 | 1.68 ± 0.34 |
Sabinene | 963 | 969 | 0.05 ± 0.08 | 0.25 ± 0.06 | 0.16 ± 0.23 | 0.18 ± 0.31 | ||
Myrcene | 973 | 988 | 0.02 ± 0.03 | 0.16 ± 0.14 | ||||
β-Pinene | 974 | 974 | 0.07 ± 0.13 | 0.17 ± 0.23 | 0.30 ± 0.03 | |||
δ-3-Carene | 998 | 1008 | 0.25 ± 0.24 | 0.71 ± 1.00 | 1.77 ± 0.46 | 1.20 ± 0.23 | 0.82 ± 0.54 | |
p-Cymene | 1013 | 1020 | ||||||
Limonene | 1018 | 1024 | 0.06 ± 0.10 | 0.22 ± 0.15 | 0.16 ± 0.03 | 0.30 ± 0.23 | ||
(Z)-β-Ocimene | 1033 | 1032 | 0.05 ± 0.09 | 0.26 ± 0.29 | 0.58 ± 0.06 | 0.86 ± 0.30 | 0.68 ± 0.19 | |
(E)-β-Ocimene | 1043 | 1044 | 0.05 ± 0.09 | 0.08 ± 0.14 | 0.34 ± 0.06 | 0.77 ± 0.21 | 0.57 ± 0.24 | |
p-Mentha-2,4(8)-diene | 1074 | 1085 | 0.04 ± 0.04 | 0.05 ± 0.04 | ||||
Linalool | 1090 | 1095 | 0.07 ± 0.06 | |||||
allo-Ocimene | 1119 | 1128 | 0.09 ± 0.01 | 0.09 ± 0.13 | 0.79 ± 1.32 | |||
Camphor | 1138 | 1141 | 0.49 ± 0.30 | 0.10 ± 0.10 | 0.43 ± 0.52 | 1.28 ± 0.66 | 1.34 ± 1.89 | 0.11 ± 0.03 |
Camphene hydrate | 1147 | 1145 | 0.01 ± 0.02 | 0.04 ± 0.04 | 0.06 ± 0.08 | 0.09 ± 0.02 | ||
Isoborneol | 1147 | 1155 | 0.12 ± 0.21 | 0.15 ± 0.26 | 0.62 ± 0.29 | 0.43 ± 0.60 | 0.39 ± 0.13 | |
Borneol | 1156 | 1165 | 0.06 ± 0.11 | 0.06 ± 0.05 | 0.06 ± 0.08 | 0.04 ± 0.04 | ||
Citral | 1170 | 1174 | 0.04 ± 0.06 | 0.02 ± 0.03 | ||||
Terpinen-4-ol | 1172 | 1174 | 0.04 ± 0.03 | |||||
α-Terpineol | 1187 | 1186 | 0.02 ± 0.03 | 0.04 ± 0.08 | 0.13 ± 0.04 | 0.14 ± 0.00 | 0.16 ± 0.02 | |
Piperitone | 1246 | 1249 | 0.06 ± 0.10 | 0.14 ± 0.09 | 0.04 ± 0.06 | 0.08 ± 0.14 | ||
Safrole | 1282 | 1285 | 0.05 ± 0.04 | 0.06 ± 0.05 | 0.10 ± 0.12 | 0.07 ± 0.01 | 0.22 ± 0.15 | |
δ-Elemene | 1333 | 1335 | 0.11 ± 0.04 | 0.13 ± 0.16 | 0.52 ± 0.26 | 0.36 ± 0.25 | 0.40 ± 0.23 | 0.29 ± 0.04 |
α-Cubebene | 1342 | 1345 | 0.04 ± 0.03 | 0.06 ± 0.07 | 0.03 ± 0.04 | 0.02 ± 0.03 | ||
Cyclosativene | 1365 | 1369 | 0.17 ± 0.14 | 0.42 ± 0.10 | 0.28 ± 0.17 | 0.34 ± 0.03 | 0.32 ± 0.03 | |
α-Copaene | 1372 | 1374 | 1.20 ± 0.51 | 0.30 ± 0.12 | 2.35 ± 0.32 | 1.34 ± 0.62 | 1.91 ± 0.22 | 1.63 ± 0.24 |
β-Cubebene | 1385 | 1387 | 0.12 ± 0.11 | 0.27 ± 0.12 | ||||
β-Elemene | 1386 | 1389 | 0.26 ± 0.19 | 0.02 ± 0.03 | 0.59 ± 0.18 | 0.65 ± 0.41 | 0.34 ± 0.18 | 0.58 ± 0.08 |
cis-α-Bergamotene | 1411 | 1411 | 0.01 ± 0.01 | |||||
β-Caryophyllene | 1416 | 1417 | 1.50 ± 0.39 | 0.53 ± 0.16 | 3.00 ± 0.09 | 2.35 ± 1.01 | 1.93 ± 0.27 | 2.03 ± 0.08 |
β-Copaene | 1427 | 1430 | 0.22 ± 0.23 | 0.08 ± 0.08 | 0.99 ± 0.08 | 0.70 ± 0.36 | 0.60 ± 0.16 | 0.64 ± 0.05 |
γ-Muurolene | 1428 | 1478 | 0.21 ± 0.36 | |||||
trans-α-Bergamotene | 1430 | 1432 | 0.02 ± 0.03 | 0.08 ± 0.04 | 0.07 ± 0.08 | 0.03 ± 0.04 | 0.05 ± 0.04 | |
Aromadendrene | 1435 | 1439 | 0.03 ± 0.05 | 0.03 ± 0.05 | ||||
cis-Muurola-3,5-diene | 1442 | 1448 | 0.02 ± 0.03 | 0.04 ± 0.06 | ||||
6,9-Guaiadiene | 1443 | 1442 | 0.16 ± 0.10 | 0.13 ± 0.09 | 0.14 ± 0.02 | |||
trans-Muurola-3,5-diene | 1445 | 1451 | 0.02 ± 0.03 | 0.03 ± 0.03 | 0.02 ± 0.03 | |||
allo-Aromadendrene | 1448 | 1458 | 0.05 ± 0.07 | 0.06 ± 0.01 | ||||
α-Humulene | 1452 | 1452 | 0.40 ± 0.21 | 0.15 ± 0.08 | 0.90 ± 0.38 | 0.83 ± 0.50 | 0.69 ± 0.22 | 0.72 ± 0.04 |
(E)-β-Farnesene | 1452 | 1454 | 0.14 ± 0.24 | |||||
β-Santalene | 1456 | 1457 | 0.06 ± 0.06 | 0.17 ± 0.09 | 0.18 ± 0.11 | 0.11 ± 0.04 | 0.13 ± 0.01 | |
trans-Cadina-1(6),4-diene | 1469 | 1475 | 0.02 ± 0.04 | 0.06 ± 0.05 | 1.34 ± 1.68 | |||
α-Neocallitropsene | 1472 | 1474 | 0.08 ± 0.01 | 0.03 ± 0.05 | ||||
γ-Curcumene | 1476 | 1481 | 0.68 ± 1.12 | 0.05 ± 0.05 | ||||
Germacrene D | 1477 | 1484 | 1.16 ± 0.58 | 0.37 ± 0.16 | 1.39 ± 1.23 | 1.60 ± 0.67 | 1.59 ± 0.48 | 1.64 ± 0.12 |
β-Selinene | 1486 | 1489 | 0.05 ± 0.05 | |||||
γ-Muurolene | 1488 | 1478 | 0.03 ± 0.05 | |||||
trans-Muurola-4(14),5-diene | 1489 | 1493 | 0.05 ± 0.08 | 0.11 ± 0.06 | 0.05 ± 0.04 | |||
α-Selinene | 1492 | 1498 | 0.03 ± 0.05 | 0.06 ± 0.10 | ||||
Bicyclogermacrene | 1492 | 1500 | 0.04 ± 0.06 | 0.19 ± 0.22 | 0.42 ± 0.27 | 0.22 ± 0.13 | 0.25 ± 0.02 | |
α-Muurolene | 1495 | 1500 | 0.10 ± 0.09 | 0.29 ± 0.07 | 0.26 ± 0.13 | 0.20 ± 0.04 | 0.23 ± 0.03 | |
Pentadecane | 1499 | 1500 | 0.21 ± 0.09 | 0.15 ± 0.12 | 0.41 ± 0.07 | 0.23 ± 0.10 | 0.19 ± 0.02 | 0.27 ± 0.06 |
β-Bisabolene | 1505 | 1505 | 0.02 ± 0.03 | 0.08 ± 0.07 | 0.08 ± 0.09 | 0.07 ± 0.02 | 0.13 ± 0.06 | |
β-Curcumene | 1507 | 1514 | 0.02 ± 0.03 | 0.06 ± 0.07 | 0.10 ± 0.06 | 0.03 ± 0.04 | 0.04 ± 0.03 | |
γ-Cadinene | 1510 | 1513 | 0.02 ± 0.04 | 0.05 ± 0.05 | ||||
Cubebol | 1513 | 1514 | 0.18 ± 0.31 | 0.28 ± 0.39 | ||||
α-Cadinene | 1515 | 1537 | 0.28 ± 0.12 | 0.05 ± 0.05 | 0.28 ± 0.48 | 0.39 ± 0.42 | ||
Myristicin | 1519 | 1517 | 17.45 ± 2.09 | 10.52 ± 2.95 | 18.38 ± 1.01 | 19.93 ± 1.13 | 19.25 ± 1.46 | 18.47 ± 0.91 |
(E)-γ-Bisabolene | 1524 | 1529 | 0.05 ± 0.05 | 0.03 ± 0.05 | 0.03 ± 0.04 | 0.02 ± 0.03 | ||
trans-Cadina-1.4-diene | 1529 | 1533 | 0.04 ± 0.04 | 0.10 ± 0.05 | 0.03 ± 0.04 | 0.05 ± 0.05 | ||
α-Cadinene | 1535 | 1537 | 0.02 ± 0.03 | |||||
α-Copaen-11-ol | 1539 | 1539 | 0.03 ± 0.05 | 0.14 ± 0.14 | 0.28 ± 0.09 | 0.16 ± 0.11 | 0.20 ± 0.08 | |
Elemicin | 1545 | 1555 | 2.23 ± 1.16 | 0.28 ± 0.36 | 2.22 ± 0.33 | 3.13 ± 0.43 | 3.56 ± 1.06 | 3.92 ± 0.75 |
(E)-Nerolidol | 1559 | 1561 | 0.06 ± 0.06 | 0.13 ± 0.11 | 0.35 ± 0.22 | 0.17 ± 0.24 | 0.27 ± 0.10 | |
Spathulenol | 1573 | 1577 | 0.08 ± 0.09 | |||||
Germacrene D-4-ol | 1574 | 1574 | 0.05 ± 0.07 | |||||
Caryophyllene oxide | 1575 | 1582 | 0.02 ± 0.03 | 0.06 ± 0.05 | 0.19 ± 0.12 | 0.08 ± 0.01 | 0.07 ± 0.02 | |
6-Methoxyelemicin | 1579 | 1595 | 0.02 ± 0.03 | 0.21 ± 0.14 | 0.18 ± 0.25 | 0.35 ± 0.18 | ||
Viridiflorol | 1592 | 1592 | 0.06 ± 0.10 | |||||
Humulene epoxide II | 1607 | 1608 | 0.02 ± 0.03 | |||||
Dillapiole | 1618 | 1620 | 71.65 ± 7.30 | 84.65 ± 2.66 | 61.12 ± 6.71 | 54.15 ± 6.56 | 54.27 ± 5.32 | 51.96 ± 5.88 |
1-epi-Cubenol | 1627 | 1627 | 0.13 ± 0.12 | |||||
Muurola-4,10(14)-dien-1-β-ol | 1636 | 1630 | 0.15 ± 0.25 | |||||
α-epi-Muurolol | 1649 | 1640 | 0.08 ± 0.09 | |||||
α-Cadinol | 1660 | 1652 | 0.01 ± 0.02 | 0.06 ± 0.07 | 0.02 ± 0.03 | |||
Apiole | 1670 | 1677 | 0.64 ± 0.40 | 0.06 ± 0.11 | 0.85 ± 0.37 | 1.72 ± 0.68 | 1.59 ± 0.78 | 1.78 ± 0.37 |
Monoterpene hydrocarbons | 0.74 ± 0.84 | 0.09 ± 0.16 | 2.35 ± 2.78 | 5.84 ± 1.70 | 6.45 ± 2.13 | 5.70 ± 3.34 | ||
Oxygenated monoterpenes | 0.63 ± 0.54 | 0.10 ± 0.10 | 0.75 ± 1.09 | 2.27 ± 1.17 | 2.11 ± 2.77 | 0.93 ± 3.34 | ||
Sesquiterpene hydrocarbons | 5.84 ± 3.18 | 1.63 ± 0.84 | 12.67 ± 5.73 | 10.35 ± 5.79 | 9.05 ± 2.51 | 10.41 ± 2.82 | ||
Oxygenated sesquiterpenes | 0.13 ± 0.17 | 0.52 ± 0.48 | 1.56 ± 1.51 | 0.77 ± 0.86 | 0.63 ± 0.24 | |||
Phenylpropanoids | 92.04 ± 11.02 | 95.51 ± 6.08 | 82.63 ± 8.47 | 79.24 ± 9.06 | 78.92 ± 8.88 | 76.70 ± 8.24 | ||
Others | 0.21 ± 0.09 | 2.58 ± 1.30 | 0.41 ± 0.07 | 0.33 ± 0.20 | 0.22 ± 0.06 | 0.41 ± 0.10 | ||
Total | 99.59 ± 15.84 | 99.91 ± 8.48 | 99.33 ± 18.62 | 99.59 ± 19.43 | 97.52 ± 17.21 | 94.78 ± 18.08 |