Carbon# | 13C NMR | 1H NMR | Reported13C NMR | Reported1H NMR |
---|---|---|---|---|
1 | 63.8 (CH2) | 4.3, bs | 63.7(CH2) | 4.2, dd |
2 | 131.6 (CH) | 6.2, dt | 132.8(CH) | 6.1, dt |
3 | 128.9 (CH) | 6.9, d | 129.3(CH) | 6.9 dt |
4 | 136.1 (Q) | -- | 137.2(Q) | -- |
5 | 128.0 (CH) | 7.2, Overlap | 128.6(CH) | 7.2, d |
6 | 135.9 (Q) | -- | 137.0(Q) | -- |
7 | 128.7(CH) | 7.07, dd | 129.7(CH) | 7.07 dd |
8 | 126.6 (CH) | 7.05, dd | 128.0(CH) | 7.05, d |
9 | 138.6 (Q) | -- | 140.2 (Q) | -- |
10 | 37.3 (CH) | 3.1, m | 39.8(CH) | 3.08, dq |
11 | 74.6 (CH) | 4.1, m | 76.6(CH) | 4.2, dd |
12 | 48.5(CH) | 2.5, m | 51.2(CH) | 2.3, qd |
13 | 214 (Q) | -- | 214.2 (Q) | -- |
14 | 29.3 (CH3) | 2.1, s | 28.4(CH3) | 2.05, s |
15 | 21.1(CH3) | 2.3, s | 21.0 (CH3) | 2.2, s |
16 | 17.5(CH3) | 1.3, d | 19.2(CH3) | 1.2, d |
17 | 10.8(CH3) | 1.09, d | 9.7(CH3) | 0.9, d |